Plastics — Determination of dynamic mechanical properties — Part 5: Flexural vibration — Non-resonance method

This document describes a flexural, non-resonance method for determining the components of the flexural complex modulus Ef* of polymers at frequencies typically in the range 0,01 Hz to 100 Hz. Higher-frequency measurements can be made, but significant errors in the dynamic properties measured are likely to result (see 10.2.2 and 10.2.3). The method is suitable for measuring dynamic storage moduli in the range 10 MPa to 200 GPa. NOTE Although materials with moduli less than 10 MPa can be studied, more accurate measurements of their dynamic-mechanical properties can be made using shear modes of deformation (see ISO 6721-6). This method is particularly suited to the measurement of loss factors greater than 0,02 and can therefore be conveniently used to study the variation of dynamic properties with temperature and frequency through most of the glass-rubber relaxation region (see ISO 6721‑1). The availability of data determined over wide ranges of both frequency and temperature enables master plots to be derived, using frequency/temperature shift procedures, which present dynamic properties over an extended frequency range at different temperatures.

Plastiques — Détermination des propriétés mécaniques dynamiques — Partie 5: Vibration en flexion — Méthode hors résonance

General Information

Status
Published
Publication Date
16-Apr-2019
Current Stage
9020 - International Standard under periodical review
Start Date
15-Jan-2024
Completion Date
15-Jan-2024
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ISO 6721-5:2019 - Plastics -- Determination of dynamic mechanical properties
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Standards Content (Sample)

INTERNATIONAL ISO
STANDARD 6721-5
Second edition
2019-04
Plastics — Determination of dynamic
mechanical properties —
Part 5:
Flexural vibration — Non-resonance
method
Plastiques — Détermination des propriétés mécaniques
dynamiques —
Partie 5: Vibration en flexion — Méthode hors résonance
Reference number
ISO 6721-5:2019(E)
©
ISO 2019

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ISO 6721-5:2019(E)

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Published in Switzerland
ii © ISO 2019 – All rights reserved

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ISO 6721-5:2019(E)

Contents Page
Foreword .iv
1 Scope . 1
2 Normative references . 1
3 Terms and definitions . 1
4 Principle . 1
5 Apparatus . 2
5.1 Loading assembly . 2
5.1.1 General. 2
5.1.2 Load stage . 2
5.1.3 Transducers. 2
5.2 Electronic data-processing equipment . 3
5.3 Temperature measurement and control . 3
5.4 Devices for measuring test specimen dimensions . 3
6 Test specimens. 3
6.1 General . 3
6.2 Shape and dimensions . 3
6.3 Preparation . 3
7 Number of specimens . 3
8 Conditioning .
...

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