EN 13516:2001

2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.Footwear - Test methods for uppers, lining and insocks - Colour fastness to rubbingSchuhe - Prüfverfahren für Obermaterialien, Futter und Decksohlen - Farbechtheit bei AbriebChaussures - Méthodes d'essai des tiges, de la doublure et des garnitures intérieures - Stabilité de la couleur au frottementFootwear - Test methods for uppers, lining and insocks - Colour fastness to rubbing61.060ObuvalaFootwearICS:Ta slovenski standard je istoveten z:EN 13516:2001SIST EN 13516:2004en01-januar-2004SIST EN 13516:2004SLOVENSKI
STANDARD



SIST EN 13516:2004



EUROPEAN STANDARDNORME EUROPÉENNEEUROPÄISCHE NORMEN 13516December 2001ICS 61.060English versionFootwear - Test methods for uppers, lining and insocks - Colourfastness to rubbingChaussures - Méthodes d'essai des tiges, de la doublure etdes garnitures intérieures - Stabilité de la couleur aufrottementSchuhe - Prüfverfahren für Schäfte, Futter undDeckbrandsohlen - Farbechtheit bei AbriebThis European Standard was approved by CEN on 16 November 2001.CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this EuropeanStandard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such nationalstandards may be obtained on application to the Management Centre or to any CEN member.This European Standard exists in three official versions (English, French, German). A version in any other language made by translationunder the responsibility of a CEN member into its own language and notified to the Management Centre has the same status as the officialversions.CEN members are the national standards bodies of Austria, Belgium, Czech Republic, Denmark, Finland, France, Germany, Greece,Iceland, Ireland, Italy, Luxembourg, Netherlands, Norway, Portugal, Spain, Sweden, Switzerland and United Kingdom.EUROPEAN COMMITTEE FOR STANDARDIZATIONCOMITÉ EUROPÉEN DE NORMALISATIONEUROPÄISCHES KOMITEE FÜR NORMUNGManagement Centre: rue de Stassart, 36
B-1050 Brussels© 2001 CENAll rights of exploitation in any form and by any means reservedworldwide for CEN national Members.Ref. No. EN 13516:2001 ESIST EN 13516:2004



EN 13516:2001 (E)2ContentspageForeword.31Scope.42Normative references.43Terms and definitions.44Apparatus and material.54.1Method A.54.2Method B.64.3Method C.75Sampling and conditioning.75.1Method A.75.2Method B.85.3Method C.86Test method.96.1Principle.96.1.1Methods A and B.96.1.2Method C.96.2Procedure.96.2.1Method A.96.2.2Method B.116.2.3Method C.127Test report.137.1Methods A and B.137.2Method C.13Annex A.14A.1Summary of test conditions normally used for method B.14A.2Drying of pads and test specimens.14A.3Avoiding thermal damage.14Bibliography.15SIST EN 13516:2004



EN 13516:2001 (E)3ForewordThis European Standard has been prepared by Technical Committee CEN/TC 309 "Footwear", the secretariat ofwhich is held by AENOR.This European Standard shall be given the status of a national standard, either by publication of an identical text orby endorsement, at the latest by June 2002, and conflicting national standards shall be withdrawn at the latest byJune 2002.Method A of this draft European Standard is based on the IULTCS/IUF 450 method (ISO 11640:1993 "Leather;tests for colour fastness; colour fastness to cycles of to-and-fro rubbing"), and method C is based on theIULTCS/IUF 426 method (ISO 11641:1993 " Leather; tests for colour fastness; colour fastness to perspiration").Annex A is informative.This standard includes a Bibliography.According to the CEN/CENELEC Internal Regulations, the national standards organizations of the followingcountries are bound to implement this European Standard: Austria, Belgium, Czech Republic, Denmark, Finland,France, Germany, Greece, Iceland, Ireland, Italy, Luxembourg, Netherlands, Norway, Portugal, Spain, Sweden,Switzerland and the United Kingdom.SIST EN 13516:2004



EN 13516:2001 (E)41 Scope1.1 This standard specifies two test methods (method A and method B) for assessing the degree of damage(marring) and transfer of a material’s surface colour during mild dry or wet abrasion. The methods are applicable toall footwear upper, lining and insock irrespective of the material, in order to assess the suitability for the end use.1.2 This standard also specifies a method (method C) for determining the likelihood of colour bleeding frommaterials and components such as sewing threads and shoe laces due to the action of water and artificialperspiration solutions, in order to assess the suitability for the end use.2 Normative referencesThis European Standard incorporates by dated or undated reference, provisions from other publications. Thesenormative references are cited at the appropriate places in the text, and the publications are listed hereafter. Fordated references, subsequent amendments to or revisions of any of these publications apply to this EuropeanStandard only when incorporated in it by amendment or revision. For undated references, the latest edition of thepublication referred to applies (including amendments).EN 12222, Footwear - Standard atmospheres for conditioning and testing of footwear and components forfootwear.EN ISO 105-A01, Textiles - Tests for colour fastness - Part A01: General principles of testing (ISO 105-A01:1994).EN 20105-A02, Textiles - Tests for colour fastness - Part A02: Grey scale for assessing change in colour (ISO 105-A02:1993).EN 20105-A03, Textiles - Tests for colour fastness - Part A03: Grey scale for assessing staining (ISO 105-A03:1993).EN ISO 3696, Water for analytical laboratory use - Specification and test methods (ISO 3696:1987).ISO 105-F10, Textiles - Tests for colour fastness - Part F10: Specification for adjacent fabric: Multifibre.3 Terms and definitionsFor the purposes of this European Standard, the following terms and definitions apply.3.1colour fastness to rubbingresistance of a material to damage (marring) and transfer of the materials surface colour during mild dry or wetabrasion3.2perspiration fastnessresistance of a material to colour bleed when exposed to an artificial perspiration solution3.3thick leatherleather with a thickness greater than 2 mmSIST EN 13516:2004



EN 13516:2001 (E)54 Apparatus and materialThe following apparatus and material shall be used:4.1 Method A4.1.1Test machine with the following:4.1.1.1Flat horizontal metal platform of minimum dimensions 80 mm
25 mm.4.1.1.2Means of moving the platform in a direction parallel to its 80 mm edges through distance of 35 mm ± 2mm and back again at a rate of 40 cycles/min ± 2 cycles/min.4.1.1.3Pair of clamps positioned at the ends of the platform at 90° to the 80 mm edges and which aredesigned to clamp the test specimen against the platform. The clamp faces shall be a minimum distance of 80 mmapart.4.1.1.4Means of moving the clamps apart so that the test specimen is extended linearly by an amountadjustable up to 20 %.4.1.1.5Rubbing finger with a flat horizontal lower surface capable of holding a square felt pad (4.1.2). Formachines with a platform wider than 25 mm the relative position of the rubbing finger shall be adjustable across thewidth of the platform.4.1.1.6Means of holding a square felt pad (4.1.2) on the lower surface of the finger.4.1.1.7Means of applying a downward force of 4,9 N
0,1 N and 9,8 N ± 0,2 N to the rubbing finger.4.1.1.8Means of counting the number of cycles traversed by the platform.4.1.2Square pads of scoured pure wool felt with the following requirements:4.1.2.1Sides of length 15 mm ± 1 mm.4.1.2.2Mass per unit area of 1750 g/m2 ± 100 g/m2 and thickness 5,5 mm ± 0,5 mm when measured using adial gauge exerting a downward pressure of 49 kPa
5 kPa on a measuring foot diameter of 10 mm
1 mm.4.1.2.3The pH of an aqueous extract, made by shaking 5 g of ground felt in 100 ml of distilled or deionizedwater complying with EN ISO 3696 in a polyethylene bottle and leaving for 2 h, between 6 and 7.4.1.3Grey scales for assessing change in colour and staining with half step ratings conforming to EN 20105-A02and EN 20105-A034.1.4Assessment cabinet with artificial lighting as specified in EN ISO 105-A01. Alternatively, the assessmentcan be carried out in daylight from the north, when the test is carried out in the northern hemisphere, or daylightfrom the south when testing in the southern hemisphere.4.1.5Distilled or de-mineralized water complying with grade 3 of EN ISO 3696.4.1.6Synthetic perspiration solution containing per litre of solution;- Sodium chloride, 5,0 g per litre of solution, g/cm3.- Ammonia solution, density 0,880 g/cm3, 6,0 cm3.4.1.7White spirit, general purpose reagent grade.SIST EN 13516:2004



EN 13516:2001 (E)64.2 Method B4.2.1Test machine with the following:4.2.1.1Rigid horizontal platform (preferably metal) capable of clamping the test specimen.4.2.1.2Vertical rotating spindle capable of holding the circular felt pad.4.2.1.3Means of rotating the felt pad at a speed of 15,6 rad/s ± 0,5 rad/s1) .4.2.1.4Means of loading the rotating felt pad with a force of either 24,5 N
± 0,5 N and 7,1 N ± 0,2 N.4.2.1.5Means of counting the number of revolutions of the felt pad.4.2.2Circular pads of scoured pure wool felt with central holes, with the following requirements:a) Outside diameter 25 mm ± 1 mm, bore diameter 3 mm ± 0,5 mm.b) Thickness, to be measured by one of the following methods:ThicknessDownward pressure/presser foot sizeSpecimen6,5 ± 0,549 kPa ± 5 kPa/10 mm ± 1 mmCut pads or uncut sheet material5,0 ± 0,52,0 kPa ± 0,2 kPa/19 mm ± 10 mmCut padsc) Density 190 kg/m3 ± 20 kg/m3.4.2.3Grey scales for assessing the change in colour and degree of staining complying with EN 20105-A02 andEN 20105-A03 respectively.4.2.4Metal plate approximately 75 mm
65 mm and thickness 5 mm with a hole diameter 25 mm through itscentre for use in the wetting from the back with organic solvents test described in 6.2.2.6.4.2.5Polished aluminium disc (diameter approximately 50 mm and thickness approximately 12 mm) to help coolthe test specimen in dry rub tests.4.2.6Balance, capable of weighing masses up to 5 g to an accuracy of 10 mg.4.2.7Assessment cabinet with artificial lighting as specified in EN ISO 105-A01. Alternatively, the assessmentcan be carried out in daylight from the north, when the test is carried out in the northern hemisphere, or daylightfrom the south when testing in the southern hemisphere.4.2.8Distilled or deionised water complying with grade 3 of EN ISO 3696 for the wet rub test described in6.2.2.3.4.2.9Synthetic perspiration solution, for the perspiration rub test described in 6.2.2.4, consisting of:- Sodium chloride, 5 g per litre of solution, g/cm3.- Ammonia solution, density 0,880 g/cm3, 6,0 cm3.4.2.10White spirit for the spirit rub test described in 6.2.2.5.4.2.11Organic solvents (as used for solvent activated stiffeners) for the wetting from the back with organicsolvents test described in 6.2.2.6.
1)1 rad
0,16 rev.SIST EN 13516:2004



EN 13516:2001 (E)74.3 Method C4.3.1Petri dish large enough to accommodate a glass plate (4.3.2) for each test specimen assembly.4.3.2Glass plate of length at least 110 mm and width at least 55 mm with a mass of 100 g ± 2 g for each testspecimen assembly.4.3.3Rectangular pieces of multifibre fabric type DW as specified in ISO 105-F10 of dimensions 100 mm ± 5 mm 50 mm ± 2 mm.4.3.4Oven maintained at a temperature of 37 C ± 2 C.4.3.5Grey scales for assessing change in colour and staining with half steps as described in EN 20105-A02 andEN 20105-A03.4.3.6Assessment cabinet with artificial lighting as specified in EN ISO 105-A01. Alternatively, the assessmentcan be carried out in daylight from the north, when the test is carried out in the northern hemisphere, or daylightfrom the south when testing in the southern hemisphere.4.3.7Balance capable of measuring mass up to 100 g to the nearest 0,1 g for testing yarns or loose fibres.4.3.8Distilled or de-mineralized water complying with grade 3 of EN ISO 3696.4.3.9Alkaline perspiration solution containing, per litre of solution;- l-histidine monohydrochloride monohydrate:5,00 g.- Sodium chloride:5,00 g.- Disodium hydrogen orthophosphate dihydrate:2,50 g.After preparation, the solution is brought to pH 8 with 0,1 M sodium hydroxide solution.Store the solution at 4 C ± 1 C. If the solution is more than one week old check its pH and adjust as necessarybefore use. Discard the solution if precipitated solids develop.4.3.10Acid perspiration solution containing, per litre of solution;- l-histidine monohydrochloride monohydrate:5,00 g.- Sodium chloride:5,00 g.- Sodium dihydrogen orthophosphate dihydrate: 2,20 g.After preparation, the solution is brought to pH 5,5 with 0,1 M sodium hydroxide solution.Store the solution at 4 ºC ± 1 ºC. If the solution is more than one week old, check its pH and adjust as necessarybefore use. Discard the solution if precipitated solids develop.5 Sampling and conditioning5.1 Method A5.1.1Rectangular test specimens of sufficient size to be clamped firmly on the test platform (4.1.1.1) arerequired. The test specimens can be cut
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