Leather - Chemical determination of chromic oxide content - Part 3: Quantification by atomic absorption spectrometry (ISO 5398-3:2007)

This part of ISO 5398 describes a method for the determination of chromium in aqueous solution obtained from leather. This is an analysis for total chromium in leather; it is not compound specific or specific to its oxidation state. This method describes the determination of chromium by atomic absorption spectrometry and is applicable to leathers which are expected to have chromic oxide contents in excess of 5 mg/kg. Two techniques for the preparation of the solution to be analysed are included. In the case of dispute, the wet oxidation technique is to be used.

Leder - Chemische Bestimmung des Chromoxidgehaltes - Teil 3: Bestimmung durch Atomabsorptionsspektroskopie (ISO 5398-3:2007)

Der vorliegende Teil der ISO 5398 beschreibt ein Verfahren zur Bestimmung von Chrom in einer aus Leder erhaltenen wässrigen Lösung. Im vorliegenden Fall handelt es sich um eine Analyse des Gesamt-chromgehaltes in Leder, die nicht verbindungsspezifisch oder spezifisch für die Oxidationsstufe ist.
Dieses Verfahren beschreibt die Bestimmung von Chrom durch Atomabsorptionsspektrometrie und ist vorgesehen für Leder, bei denen Chromoxidgehalte von mehr als 5 mg/kg vermutet werden. Enthalten sind zwei Verfahren zur Herstellung der zu analysierenden Lösung. Im Streitfall ist das Nassoxidationsverfahren anzuwenden.

Cuir - Dosage de l'oxyde de chrome - Partie 3: Quantification par spectrométrie d'absorption atomique (ISO 5398-3:2007)

L'ISO 5398-3:2007 spécifie une méthode permettant de doser le chrome dans une solution aqueuse obtenue à partir de cuir. C'est une analyse du chrome total dans le cuir; elle est non spécifique du composé ou de son degré d'oxydation.
La présente méthode indique comment doser le chrome par spectrométrie d'absorption atomique et elle s'applique aux cuirs susceptibles de contenir de l'oxyde de chrome dans des proportions supérieures à 5 mg/kg. Deux techniques de préparation de la solution à analyser sont décrites. En cas de désaccord, c'est la méthode d'oxydation en milieu humide qui doit être utilisée.

Usnje - Kemijsko določevanje kromovega oksida - 3. del: Kvantitativno določevanje z atomsko absorpcijsko spektrometrijo (ISO 5398-3:2007)

General Information

Status
Withdrawn
Publication Date
26-Nov-2008
Withdrawal Date
29-Aug-2018
Technical Committee
Current Stage
9900 - Withdrawal (Adopted Project)
Start Date
30-Aug-2018
Due Date
22-Sep-2018
Completion Date
30-Aug-2018

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Standards Content (Sample)

SLOVENSKI STANDARD
SIST EN ISO 5398-3:2009
01-januar-2009
8VQMH.HPLMVNRGRORþHYDQMHNURPRYHJDRNVLGDGHO.YDQWLWDWLYQR
GRORþHYDQMH]DWRPVNRDEVRUSFLMVNRVSHNWURPHWULMR ,62
Leather - Chemical determination of chromic oxide content - Part 3: Quantification by
atomic absorption spectrometry (ISO 5398-3:2007)
Leder - Chemische Bestimmung des Chromoxidgehaltes - Teil 3: Bestimmung durch
Atomabsorptionsspektroskopie (ISO 5398-3:2007)
Cuir - Dosage de l'oxyde de chrome - Partie 3: Quantification par spectrométrie
d'absorption atomique (ISO 5398-3:2007)
Ta slovenski standard je istoveten z: EN ISO 5398-3:2007
ICS:
59.140.30 Usnje in krzno Leather and furs
SIST EN ISO 5398-3:2009 en,fr,de
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

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SIST EN ISO 5398-3:2009

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SIST EN ISO 5398-3:2009
EUROPEAN STANDARD
EN ISO 5398-3
NORME EUROPÉENNE
EUROPÄISCHE NORM
August 2007
ICS 59.140.30

English Version
Leather - Chemical determination of chromic oxide content - Part
3: Quantification by atomic absorption spectrometry (ISO 5398-
3:2007)
Cuir - Dosage chimique de l'oxyde de chrome - Partie 3: Leder - Chemische Bestimmung des Chromoxidgehalts -
Quantification par spectrométrie d'absorption atomique Teil 3: Bestimmung durch Atomabsorptionsspektrometrie
(ISO 5398-3:2007) (ISO 5398-3:2007)
This European Standard was approved by CEN on 28 July 2007.
CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this European
Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such national
standards may be obtained on application to the CEN Management Centre or to any CEN member.
This European Standard exists in three official versions (English, French, German). A version in any other language made by translation
under the responsibility of a CEN member into its own language and notified to the CEN Management Centre has the same status as the
official versions.
CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Cyprus, Czech Republic, Denmark, Estonia, Finland,
France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal,
Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland and United Kingdom.
EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION
EUROPÄISCHES KOMITEE FÜR NORMUNG
Management Centre: rue de Stassart, 36  B-1050 Brussels
© 2007 CEN All rights of exploitation in any form and by any means reserved Ref. No. EN ISO 5398-3:2007: E
worldwide for CEN national Members.

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SIST EN ISO 5398-3:2009
EN ISO 5398-3:2007 (E)
Contents Page
Foreword.3

2

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SIST EN ISO 5398-3:2009
EN ISO 5398-3:2007 (E)
Foreword
This document (EN ISO 5398-3:2007) has been prepared by Technical Committee CEN/TC 289 "Leather", the
secretariat of which is held by UNI, in collaboration with the International Union of Leather Technologists and
Chemists Societies (IULTCS).
This European Standard shall be given the status of a national standard, either by publication of an identical
text or by endorsement, at the latest by February 2008, and conflicting national standards shall be withdrawn
at the latest by February 2008.
According to the CEN/CENELEC Internal Regulations, the national standards organizations of the following
countries are bound to implement this European Standard: Austria, Belgium, Bulgaria, Cyprus, Czech
Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia,
Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain,
Sweden, Switzerland and the United Kingdom.
3

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SIST EN ISO 5398-3:2009

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SIST EN ISO 5398-3:2009

INTERNATIONAL ISO
STANDARD 5398-3
IULTCS/IUC
8:3
First edition
2007-08-01

Leather — Chemical determination of
chromic oxide content —
Part 3:
Quantification by atomic absorption
spectrometry
Cuir — Dosage chimique de l'oxyde de chrome —
Partie 3: Quantification par spectrométrie d'absorption atomique



Reference number
ISO 5398-3:2007(E)
IULTCS/IUC 8:3:2007(E)
©
ISO 2007

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SIST EN ISO 5398-3:2009
ISO 5398-3:2007(E)
IULTCS/IUC 8:3:2007(E)
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All rights reserved. Unless otherwise specified, no part of this publication may be reproduced or utilized in any form or by any means,
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ii © ISO 2007 – All rights reserved

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SIST EN ISO 5398-3:2009
ISO 5398-3:2007(E)
IULTCS/IUC 8:3:2007(E)
Contents Page
Foreword. iv
Introduction . v
1 Scope .1
2 Normative references .1
3 Terms and definitions .1
4 Principle.1
5 Sampling and sample preparation.2
6 Reagents.2
6.1 Wet oxidation method .2
6.2 Atomic absorption spectrometry .2
7 Apparatus .2
8 Methods .3
8.1 Preparation of analytical solution.3
8.2 Measurement of the aqueous solution.3
9 Calculation and expression of results.4
10 Test report .5
Annex A (informative) Determination of water and other volatile matter.6

© ISO 2007 – All rights reserved iii

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SIST EN ISO 5398-3:2009
ISO 5398-3:2007(E)
IULTCS/IUC 8:3:2007(E)
Foreword
ISO (the International Organization for Standardization) is a worldwide federation of national standards bodies
(ISO member bodies). The work of preparing International Standards is normally carried out through ISO
technical committees. Each member body interested in a subject for which a technical committee has been
established has the right to be represented on that committee. International organizations, governmental and
non-governmental, in liaison with ISO, also take part in the work. ISO collaborates closely with the
International Electrotechnical Commission (IEC) on all matters of electrotechnical standardization.
International Standards are drafted in accordance with the rules given in the ISO/IEC Directives, Part 2.
The main task of technical committees is to prepare International Standards. Draft International Standards
adopted by the technical committees are circulated to the member bodies for voting. Publication as an
International Standard requires approval by at least 75 % of the member bodies casting a vote.
Attention is drawn to the possibility that some of the elements of this document may be the subject of patent
rights. ISO shall not be held responsible for identifying any or all such patent rights.
This part of ISO 5398 was prepared by the Chemical Tests Commission of the International Union of Leather
Technologists and Chemists Societies (IUC Commission, IULTCS) in collaboration with the European
Committee for Standardization (CEN) Technical Committee CEN/TC 289, Leather, the secretariat of which is
held by UNI, in accordance with the agreement on technical co-operation between ISO and CEN (Vienna
Agreement). It is based on IUC 8 originally published in J. Soc. Leather Trades Chemists 49, p. 17, (1965)
and declared an official method of the IULTCS in 1965.
IULTCS, originally formed in 1897, is a world-wide organization of professional leather societies to further the
advancement of leather science and technology. IULTCS has three Commissions, which are responsible for
establishing international methods for the sampling and testing of leather. ISO recognizes IULTCS as an
international standardizing body for the preparation of test methods for leather.
ISO 5398 consists of the following parts, under the general title Leather — Chemical determination of chromic
oxide content:
⎯ Part 1:
...

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